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Aqueous One-Pot Synthesis of Derivatized Cyclopentadienyl-Tricarbonyl Complexes of99mTc with an In Situ CO Source: Application to a Serotonergic Receptor Ligand

  • Wald J
  • Alberto R
  • Ortner K
  • et al.
Angewandte Chemie International Edition (2001) 40(16) 3062-3066
DOI: 10.1002/1521-3773(20010817)40:16<3062::aid-anie3062>3.0.co;2-o
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Abstract

Half-sandwich complexes of the type [(RCOCp)99mTc(CO)3] (e.g. 1) were synthesized in a single step in water from [99mTcO4]−. The acidification of the Cp ring by a carbonyl substituent and the use of K2[H3BCO2] as a reducing agent and in situ source of CO are instrumental in the synthesis.

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Wald, J., Alberto, R., Ortner, K., & Candreia, L. (2001). Aqueous One-Pot Synthesis of Derivatized Cyclopentadienyl-Tricarbonyl Complexes of99mTc with an In Situ CO Source: Application to a Serotonergic Receptor Ligand. Angewandte Chemie International Edition, 40(16), 3062–3066. https://doi.org/10.1002/1521-3773(20010817)40:16<3062::aid-anie3062>3.0.co;2-o

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