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The stereochemistry of the 1,2-addition of Grignard reagents to some steroidal unsaturated ketones

Journal of Chemical Research - Part S (2003) (8) 474-476
DOI: 10.3184/030823403103174588
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Abstract

The stereochemistry of 3β,17β-dihydroxy-3α -ethylandrost-4-ene, 3α, 17β-dihydroxy-3β-methylestr-4-ene and 3β-acetoxy-7α,17β-dihydroxy-7β-methylandrost-5-ene, which were obtained by Grignard reactions from the corresponding αβ -unsaturated ketones, have been established by X-ray crystallography.

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Uyanik, C., Hanson, J. R., & Hitchcock, P. B. (2003). The stereochemistry of the 1,2-addition of Grignard reagents to some steroidal unsaturated ketones. Journal of Chemical Research - Part S, (8), 474–476. https://doi.org/10.3184/030823403103174588

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