In-depth polymerization of a self-adhesive dual-cured resin cement

Abstract

The aim of this study was to assess Knoop hardness at different depths of a dual-cured self-adhesive resin cement through different thicknesses of Empress Esthetic ® ceramic. Flattened bovine dentin was embedded in resin. The cement was inserted into a rubber mold (0.8×5 mm) that was placed between two polyvinyl chloride plastic films and placed over the flat dentin and light cured by Elipar Trilight-QTH (800 mW/cm 2) or Ultra-Lume light-emitting diode (LED 5; 1585 mW/cm 2) over ceramic disks 1.4 or 2 mm thick. The specimens (n=6) were stored for 24 hours before Knoop hardness (KHN) was measured. The data were submitted to analysis of variance in a factorial split-plot design and Tukey's test (α=0.05). There was significant interaction among the study factors. In the groups cured by the QTH unit, an increase in ceramic thickness resulted in reduced cement hardness values at all depths, with the highest values always being found in the center (1.4 mm, 58.1; 2 mm, 50.1) and the lowest values at the bottom (1.4 mm, 23.8; 2 mm, 20.2). When using the LED unit, the hardness values diminished with increased ceramic thickness only on the top (1.4 mm, 51.5; 2 mm, 42.3). In the group with the 1.4-mmthick disk, the LED curing unit resulted in similar values on the top (51.5) and center (51.9) and lower values on the bottom (24.2). However, when the cement was light cured through the 2-mm disk, the highest hardness value was obtained in the center (51.8), followed by the top (42.3) and bottom (19.9), results similar to those obtained with the QTH curing unit (center > top > bottom). The hardness values of the studied cement at different depths were dependent on the ceramic thickness but not on the light curing units used. © Operative Dentistry, 2012.