Effect of annealing temperature on the evolution of microstructure, texture, and mechanical properties of hot-rolled 12Cr-ODS steel

Abstract

To achieve high thermal efficiency, today's nuclear reactor structures are exposed to higher temperatures and pressures, which requires the use of high-strength steels with specific properties, such as ODS steels. There is a need to clarify the evolution of the microstructure and properties of steels at elevated temperatures. This study systematically investigates the evolution of microstructure, texture, and mechanical property variations of 12Cr-ODS steels after hot-rolling and subsequent annealing at 1000 °C and 1200 °C. The investigation utilizes optical microscopy, electron backscatter diffraction technique, and mechanical property measurements. The microstructure of hot-rolled samples shows a layered alternating distribution, which is distinguished by a notable presence of the α-fiber texture. Following annealing at 1000 °C, the martensite grains are smaller with a reduced hardness, while maintaining a strong α-fiber texture. After annealing at 1200 °C, there is a rapid increase in the growth of martensite grains, a significant rise in hardness, a reduction in the α-fiber texture characteristics, and an improvement in the γ-fiber texture characteristics. Moreover, the maximum intensity of the α-fiber texture diminishes as the annealing temperature increases. The mechanical properties of the samples deteriorated after annealing at 1200 °C, which can be attributed to the coarse martensite grains and the texture components containing the {001} cleavage plane dominating the occurrence of brittle cleavage fracture. The 0.1Y sample after annealing at 1000 °C exhibits an excellent combination of strength (1458 MPa) and ductility (20.3%), which is owing to the unique heterogeneous grain structure and the evolution of favorable texture.