Texture Feature Analysis of the Microstructure of Cement-Based Materials During Hydration

Abstract

This study presents a comprehensive grayscale texture analysis framework for investigating the microstructural evolution of cement-based materials during hydration. High-resolution X-ray computed tomography (X-CT) slice images were analyzed across five hydration ages (12 h, 1 d, 3 d, 7 d, and 31 d) using three complementary methods: grayscale histogram statistics, fractal dimension calculation via differential box-counting, and texture feature extraction based on the gray-level co-occurrence matrix (GLCM). The average value of the mean grayscale value of slice (MeanG_AVE) shows a trend of increasing and then decreasing. Average fractal dimension values (DB_AVE) decreased logarithmically from 2.48 (12 h) to 2.41 (31 d), quantifying progressive microstructural homogenization. The trend reflects pore refinement and gel network consolidation. GLCM texture parameters—including energy, entropy, contrast, and correlation—captured the directional statistical patterns and phase transitions during hydration. Energy increased with hydration time, reflecting greater spatial homogeneity and phase continuity, while entropy and contrast declined, signaling reduced structural complexity and interfacial sharpness. A quantitative evaluation of parameter performance based on intra-sample stability, inter-sample discrimination, and signal-to-noise ratio (SNR) revealed energy, entropy, and contrast as the most effective descriptors for tracking hydration-induced microstructural evolution. This work demonstrates a novel, integrative, and segmentation-free methodology for texture quantification, offering robust insights into the microstructural mechanisms of cement hydration. The findings provide a scalable basis for performance prediction, material optimization, and intelligent cementitious design.