Microflow photochemistry: UVC-induced [2 + 2]-photoadditions to furanone in a microcapillary reactor

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Abstract

[2 + 2]-Cycloadditions of cyclopentene and 2,3-dimethylbut-2-ene to furanone were investigated under continuous-flow conditions. Irradiations were conducted in a FEP-microcapillary module which was placed in a Rayonet chamber photoreactor equipped with low wattage UVC-lamps. Conversion rates and isolated yields were compared to analogue batch reactions in a quartz test tube. In all cases examined, the microcapillary reactor furnished faster conversions and improved product qualities. © 2013 Bachollet et al; licensee Beilstein-Institut.

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Bachollet, S., Terao, K., Aida, S., Nishiyama, Y., Kakiuchi, K., & Oelgemöller, M. (2013). Microflow photochemistry: UVC-induced [2 + 2]-photoadditions to furanone in a microcapillary reactor. Beilstein Journal of Organic Chemistry, 9, 2015–2021. https://doi.org/10.3762/bjoc.9.237

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