Analysis of 2-deuterated isopentenyl alcohols by 1H NMR of chiral esters

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Abstract

A convenient procedure is presented whereby the chirality of isopentenyl alcohols labeled with deuterium in the 2-position can be determined by1H NMR analysis of their chiral esters. The MTPA, MPA and O-acetylmandelate esters were investigated in a series of NMR solvents. The best results were obtained using the O-acetylmandelates in C6D6with homodecoupling of the 1-position. © 2002 Elsevier Science Ltd. All rights reserved.

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Giner, J. L., Kiemle, D., & Zuniga, D. J. (2002). Analysis of 2-deuterated isopentenyl alcohols by 1H NMR of chiral esters. Tetrahedron Letters, 43(7), 1175–1177. https://doi.org/10.1016/S0040-4039(01)02404-2

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