Convenient and rapid determination of the configuration of aldoximes and ketoximes by means of noe difference spectroscopy

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Abstract

Based on a through-space connection observed between the hydroxyl proton and the iminyl proton or protons attached to the α-carbon atom in various types of oximes, homonuclear NOE difference spectroscopy utilizing d6-DMSO as solvent is proposed as a simple method for the elucidation of the stereochemistry. © 1990.

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Heinisch, G., & Holzer, W. (1990). Convenient and rapid determination of the configuration of aldoximes and ketoximes by means of noe difference spectroscopy. Tetrahedron Letters, 31(22), 3109–3112. https://doi.org/10.1016/S0040-4039(00)94707-5

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