Highly chemoselective synthesis of 1,2,3,4,5-pentasubstituted cyclohexanols under solvent-free condition

  • Luo X
  • Shan Z
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Abstract

Acetophenone reacted with a series of aromatic aldehydes with grinding under catalysis of a double-component solid base system consisting of NaOH and K2CO3to furnish highly chemoselectively 1,2,3,4,5-pentasubstituted cyclohexanols in 80-95% yield, and their composition and structure are identified by spectral technologies and single crystal X-ray diffraction analysis, and a possible mechanism of the formation was suggested. © 2006 Elsevier Ltd. All rights reserved.

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Authors

  • Xinxiang Luo

  • Zixing Shan

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