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Abstract

The cyclobutadieneiron tricarbonyls I and II were prepd. from III by treatment with KR. Successive photolysis and Ce(IV) oxidn. of I gave 83% 5-methylisochroman. (IV) oxidn. of II gave 50% 4-methylphthalan. [on SciFinder(R)]

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Grubbs, R. H., Pancoast, T. A., & Grey, R. A. (1974). Intramolecular trapping of cyclobutadiene. Tetrahedron Letters, 15(28), 2425–2426. https://doi.org/10.1016/S0040-4039(01)92275-0

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