[186Re]Re(V)DMSA, a β-emitting analogue of the tumour imaging radiopharmaceutical pentavalent [99mTc]Tc(V)DMSA of possible value in tumour therapy, is readily prepared by stannous reduction of [186Re]ReO4-in the presence of dimercaptosuccinic acid at 100°C using a commercial DMSA kit as used for renal imaging with99mTc, and purified using a disposable sample preparation column. The complex has been identified as [ReO(DMSA)2]-by NMR, optical and i.r. spectroscopy and elemental analysis. © 1991.
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