Two 2D experiments, novel to solid-state NMR, are demonstrated using the trimethylsilyl ester of cubic octameric silicate (Q8M8). J-Resolved13C NMR with BLEW-12 proton homonuclear decoupling reveals the scalar13C1H couplings and29Si SUPERCOSY the connectivities of silicon atoms in the distorted Q8cube. © 1992.
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