Two-dimensional J-resolved and SUPERCOSY NMR experiments in the solid state

  • Kolodzicjski W
  • Klinowski J
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Abstract

Two 2D experiments, novel to solid-state NMR, are demonstrated using the trimethylsilyl ester of cubic octameric silicate (Q8M8). J-Resolved13C NMR with BLEW-12 proton homonuclear decoupling reveals the scalar13C1H couplings and29Si SUPERCOSY the connectivities of silicon atoms in the distorted Q8cube. © 1992.

Author-supplied keywords

  • COSY
  • J-resolved
  • Q8M8
  • solid-state NMR
  • two-dimensional NMR

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Authors

  • Waclaw Kolodzicjski

  • Jacek Klinowski

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