Variously substituted glycals are readily prepared from glycosyl bromides using (Cp2TiCl)2

  • Spencer R
  • Schwartz J
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Glycosyl halides, variously substituted with ether, acetal, or ester protecting groups, were converted to the corresponding glycals in high yield by reaction with (Cp2TiCl)2. A glycosyl chloride was less reactive than the analogous bromide.

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