Characterization of technical lignins by NMR spectroscopy: optimization of functional group analysis by 31P NMR spectroscopy

  • Korntner P
  • Sumerskii I
  • Bacher M
 et al. 
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P nuclear magnetic resonance (NMR) based on the derivatization reagent 2-chloro-4,4,5,5-tetramethyl-1,3,2-dioxaphospholane is a common approach for the hydroxyl group determination of lignins, but the results are sometimes less reproducible compared to other methods. In the present work, common pitfalls in

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  • Philipp Korntner

  • Ivan Sumerskii

  • Markus Bacher

  • Thomas Rosenau

  • Antje Potthast

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