Orange crystalline tetrabutylammonium tribromide was prepared using a simple method. The reaction of acetyl derivatives with an equimolar amount of the tribromide in dichloromethane–methanol at room temperature gave bromoacetyl derivatives in fairly good yields.
CITATION STYLE
Kajigaeshi, S., Kakinami, T., Okamoto, T., & Fujisaki, S. (1987). Synthesis of Bromoacetyl Derivatives by Use of Tetrabutylammonium Tribromide. Bulletin of the Chemical Society of Japan, 60(3), 1159–1160. https://doi.org/10.1246/bcsj.60.1159
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