Research on activated alumina obtained by spray pyrolysis method

Abstract

Activated Alumina was prepared by directly spray pyrolysis A1C13 solution. Batch experiments was performed to choose better reaction device among muffle furnace, propane graphite furnace and tubular resistance furnace. The alumina was characterized by XRD and SEM, and the specific surface area of the prepared alumina was also examined. The experiment results showed lhat using the tubular resistance furnace by spray pyrolysis AICI3 solution could effectively improve the efficiency of the pyrolysis, obviously change the morphology of product and effectively increase the specific surface area of product granule. Compared with the muffle furnace roasting, the product index of spray pyrolysis by using tubular resistance furnace was better, and the products conformed to the requirements of the index of activated alumina. The present paper provided a new way of preparing activated alumina.