The use of 13C‐NMR spectroscopy in the establishment of lipid A backbone structure from lipopolysaccharide of Yersinia pseudotuberculosis has been described. The 13C‐NMR spectra of degraded lipid A and its N‐acetate were obtained. The assignment of signals was made by comparison with the chemical shifts for 13C‐NMR spectra of glucosaminitol, N‐acetyl‐glucosaminitol and their β‐1,4 and β‐1,6 disaccharides. It was shown that lipid A backbone of the lipopolysaccharide in question consists of β‐1,6‐linked glucosamine disaccharide. Copyright © 1982, Wiley Blackwell. All rights reserved
CITATION STYLE
KRASIKOVA, I. N., GORBACH, V. I., ISAKOV, V. V., SOLOV’EVA, T. F., & OVODOV, Y. S. (1982). The Application of 13C‐NMR Spectroscopy to Study Lipid A from Yersinia pseudotuberculosis Lipopolysaccharide. European Journal of Biochemistry, 126(2), 349–351. https://doi.org/10.1111/j.1432-1033.1982.tb06786.x
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