Validation of atomic absorption spectrophotometry and mercury analyzer for analysis of cadmium, lead and mercury in red chili pepper

13Citations
Citations of this article
28Readers
Mendeley users who have this article in their library.

Abstract

A Flame-Atomic Absorption Spectrophotometry (AAS-flame) for the quantification of cadmium (Cd) and lead (Pb) and mercury analyzer for quantitative analysis of mercury (Hg) in red chili pepper (Capsicum annum L.) were developed and validated. The method was validated for some parameters, namely linearity and range, precision, accuracy, Limit of Detection (LoD) and Limit of Quantification (LoQ), according to International Conference on Harmonization (ICH). The standard curves were linear over the concentration ranges of 0.1-1.4 μg mLG -1 (Cd), 0.10-1.80 μg mLG -1 (Pb) and 0.5-20 μg mLG -1 with correlation coefficient (r) values >0.99. The detection limits obtained were 0.022 μg mLG -1 , 0.0594 μg mLG -1 and 1.77 μg mLG -1 for Cd, Pb and Hg, respectively. The quantification limits obtained were 0.075 μg mLG -1 (Cd), 0.1981 μg mLG -1 (Cd) and 5.91 μg mLG -1 (Hg). The Relative Standard Deviation (RSD) values found for its intra-day and interday precision were lower than those required by RSD Horwitz. The mean recovery percentage was 97.98-101.9133%.The validated methods were successfully used for determination of Cd, Pb and Hg in red chili pepper.

References Powered by Scopus

Molecular and cellular mechanisms of cadmium carcinogenesis

1346Citations
N/AReaders
Get full text

Heavy metal contamination of soil and vegetables in suburban areas of Varanasi, India

806Citations
N/AReaders
Get full text

Trends in quality in the analytical laboratory. II. Analytical method validation and quality assurance

793Citations
N/AReaders
Get full text

Cited by Powered by Scopus

Performance evaluation of a novel rGO-Fe<sup>0</sup>/Fe<inf>3</inf>O<inf>4</inf>-PEI nanocomposite for lead and cadmium removal from aqueous solutions

42Citations
N/AReaders
Get full text

Development and validation of a GF-AAS method and its application for the trace level determination of Pb, Cd, and Cr in fish feed samples commonly used in the hatcheries of Bangladesh

30Citations
N/AReaders
Get full text

Assessment of heavy metals in wastewater plant effluent and lake water by using atomic absorption spectrophotometry

19Citations
N/AReaders
Get full text

Register to see more suggestions

Mendeley helps you to discover research relevant for your work.

Already have an account?

Cite

CITATION STYLE

APA

Rawar, E. A., & Rohman, A. (2016). Validation of atomic absorption spectrophotometry and mercury analyzer for analysis of cadmium, lead and mercury in red chili pepper. Asian Journal of Agricultural Research, 10(1), 65–71. https://doi.org/10.3923/ajar.2016.65.71

Readers' Seniority

Tooltip

PhD / Post grad / Masters / Doc 5

50%

Lecturer / Post doc 3

30%

Professor / Associate Prof. 2

20%

Readers' Discipline

Tooltip

Chemistry 7

58%

Pharmacology, Toxicology and Pharmaceut... 3

25%

Agricultural and Biological Sciences 1

8%

Environmental Science 1

8%

Save time finding and organizing research with Mendeley

Sign up for free