Microwave-assisted synthesis of quinoline alkaloids: 4-Methoxy-1-methyl-2-quinolinone and its analogs

  • Nadaraj V
  • Selvi S
  • Sasi R
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Abstract

The microwave-induced synthesis of some quinoline alkaloids of the type 4-methoxy-1-methyl- 2-quinolinone including folimine is reported. The precursors 4-hydroxy-2-quinolinone derivatives were effectively prepared in a single step from aniline and diethylmalonate using p- toluenesulfonic acid as a catalyst and these intermediates were converted to the titled quinoline alkaloids by treatment with dimethyl sulfate, N,N-dimethylformamide and potassium carbonate. The presented synthentic procedure is a convenient, simple and fast alternative for synthesizing 4-methoxy-1-methyl-2-quinolinone and its derivatives.

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Nadaraj, V., Selvi, S. T., & Sasi, R. (2006). Microwave-assisted synthesis of quinoline alkaloids: 4-Methoxy-1-methyl-2-quinolinone and its analogs. Arkivoc, 2006(10), 82–89. https://doi.org/10.3998/ark.5550190.0007.a11

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