Effect of ultrasonic vibration on structural and physical properties of resin-based dental composites

Abstract

This study aimed to investigate the influence of ultrasonic heat before photo-polymerization on the structural and physical properties of dental composites. Commercially available bulk-fill, nano-hybrid, micro-hybrid, and flowable composites were used. The samples were divided into three groups i.e., (i) without ultrasonic activation, (ii) ultrasonic activation at 15 Hz for 30 s, and (iii) ultrasonic activation at 15 Hz for 60 s. The degree of conversion percentage (DC%) and structural changes were evaluated with Fourier transform infrared spectroscopy. The presence of voids in restored tooth cavities were investigated with micro-computed tomography. The statistical analysis was performed using a one-way analysis of variance (ANOVA) post hoc Tukey’s test. The DC% was significantly increased with ultrasonic application in all groups except for flowable composites, whereby flowable composite showed a significant increase with 30 s ultrasonic activation only. The highest DC% was observed in 60 s ultrasonically activated nano-hybrid and micro-hybrid composites. The voids were reduced linearly with ultrasonic application in flowable and bulk-fill composites; however, non-linear behavior was observed with micro-hybrid and nano-hybrid composites, whereby the difference was significant within the groups. The frequency and time of the ultrasonic application is an important factor to consider and can be used to preheat composites before clinical application.