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Convenient Preparation of Dimethyl (Trifluoromethyl)malonate and Related Compounds

  • Ishikawa N
  • Yokozawa T
Bulletin of the Chemical Society of Japan (1983) 56(3) 724-726
DOI: 10.1246/bcsj.56.724
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Abstract

The preparative method for dimethyl (trifluoromethyl)malonate (4) from the adduct of perfluoro-2-methylpropene with methanol was improved, and several reactions of this base-sensitive substance were investigated. Alkylation of 4 was achieved by using CsF as a condensing agent, and the Michael addition on vinyl ketones proceeded in triethylamine–pyridine medium.

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Ishikawa, N., & Yokozawa, T. (1983). Convenient Preparation of Dimethyl (Trifluoromethyl)malonate and Related Compounds. Bulletin of the Chemical Society of Japan, 56(3), 724–726. https://doi.org/10.1246/bcsj.56.724

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