Electrochemical methoxylation of vinyl ethers: a novel anodic dimerization reaction

  • Belleau B
  • Au-Young Y
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Abstract

Electrolysis of vinyl ethers in methanol using a platinum anode and nickel cathode was found to yield the corresponding 1,2-dimethoxylation products (60–66%) and products resulting from a tail-to-tail dimerization to succindialdehyde acetals (20–22%). A mechanism involving radical cation intermediates is proposed.

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Belleau, B., & Au-Young, Y. K. (1969). Electrochemical methoxylation of vinyl ethers: a novel anodic dimerization reaction. Canadian Journal of Chemistry, 47(11), 2117–2118. https://doi.org/10.1139/v69-343

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