Inter-laboratory Comparison on Thermal Diffusivity Measurements by the Laser Flash Method at Ultra-high Temperature

Abstract

An inter-laboratory comparison has been performed between seven participants on thermal diffusivity measurements by the laser flash method in the temperature range from 23 °C to 3000 °C. The main objective was to assess the variability and coherency of thermal diffusivity measurements performed at ultra-high temperatures at the European level. Three refractory materials (molybdenum, tungsten and isotropic graphite IG210) were selected for this inter-laboratory comparison, due to their high melting point. The disk-shaped specimens needed were machined from the same blocks of materials in order to reduce any potential scattering of results between participants due to inhomogeneity effects. The homogeneity of the sets of specimens was studied by the pilot laboratory (LNE) before launching the comparison process. Thermal diffusivity measurements were then carried out by the seven participants on the three materials during two successive thermal cycles up to the maximum temperatures that can be reached by the devices used. The analysis of results showed a good agreement between the participants for temperatures above 400 °C, with relative deviations within the uncertainties of measurement and lower than ± 4 % for molybdenum, ± 5 % for isotropic graphite and ± 9 % for tungsten.