The reaction of diethyl bromomalonate with p-tert-Butylthiacalix[4]arene: An approach to asymmetrical derivatives

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Abstract

New dissymmetric and asymmetric p-tert-butylthiacalix[4]arene derivatives were prepared as a result of the reaction of p-tert-butylthiacalix[4]arene with diethyl bromomalonate in the presence of different alkali metals (Cs, K and Na) in refluxing acetone for 7 days. The structures of the prepared compounds were investigated by IR, 1HNMR and MALDI-TOF mass spectroscopy.

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Omran, A. (2009). The reaction of diethyl bromomalonate with p-tert-Butylthiacalix[4]arene: An approach to asymmetrical derivatives. Molecules, 14(5), 1755–1761. https://doi.org/10.3390/molecules14051755

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