Abstract
A high pressure liquid chromatographic procedure is described for assay of toxins associated with paralytic shellfish poisoning (PSP). The method is applicable to saxitoxin, neosaxitoxin, gonyautoxins I through IV, and their sulfocarbamoyl derivatives. Toxins are separated on a bonded phase cyano column and detected by fluorescence following alkaline oxidation (NH+4 and periodic acid). The utility of the HPLC procedure for research and monitoring is discussed.
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CITATION STYLE
Sullivan, J. J., & Iwaoka, W. T. (1983). High pressure liquid chromatographic determination of toxins associated with paralytic shellfish poisoning. Journal - Association of Official Analytical Chemists, 66(2), 297–303. https://doi.org/10.1093/jaoac/66.2.297
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