Silver-Triggered Activity of a Heterogeneous Palladium Catalyst in Oxidative Carbonylation Reactions

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Abstract

A silver-triggered heterogeneous Pd-catalyzed oxidative carbonylation has been developed. This heterogeneous process exhibits high efficiency and good recyclability, and was utilized for the one-pot construction of polycyclic compounds with multiple chiral centers. AgOTf was used to remove chloride ions in the heterogeneous catalyst Pd-AmP-CNC, thereby generating highly active PdII, which results in high efficiency of the heterogeneous catalytic system.

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Li, M. B., Yang, Y., Rafi, A. A., Oschmann, M., Grape, E. S., Inge, A. K., … Bäckvall, J. E. (2020). Silver-Triggered Activity of a Heterogeneous Palladium Catalyst in Oxidative Carbonylation Reactions. Angewandte Chemie - International Edition, 59(26), 10391–10395. https://doi.org/10.1002/anie.202001809

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