Electrodeposition and characterization of lanthanide elements on carbon sheets

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Abstract

Electrochemical coating and recovery by electrodeposition have been invaluably employed for facial thin film fabrication and the recycling of used materials. Herein, we have established a full data set of lanthanide (Ln: La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, and Yb) elements electrodeposited on carbon sheets. Cyclic voltammetry was performed for 10 mM Ln(III) ions in a 0.1 M NaClO4 electrolyte over a carbon sheet between +0.5 V and -1.7 V (vs. Ag/AgCl). Amperometry was performed at a given potential to electrodeposit the Ln element on the carbon sheet. Their physicochemical properties were fully investigated by scanning electron microscopy, Fouriertransform infrared spectroscopy, energy-dispersive X-ray spectroscopy, and X-ray photoelectron spectroscopy. The newly established full data set for Ln(III) ions over carbon electrodes provides useful fundamental information for the development of coating and recovery methods of Ln elements.

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Joo, M. H., Park, S. J., Hong, S. M., Rhee, C. K., Kim, D., & Sohn, Y. (2021). Electrodeposition and characterization of lanthanide elements on carbon sheets. Coatings, 11(1), 1–14. https://doi.org/10.3390/coatings11010100

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