Electrospray ionization mass spectrometric analysis of highly reactive glycosyl halides

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Abstract

Highly reactive glycosyl chlorides and bromides have been analysed by a routine mass spectrometric method using electrospray ionization and lithium salt adduct-forming agents in anhydrous acetonitrile solution, providing salient lithiated molecular ions [M+Li] +, [2M+Li] + etc. The role of other adduct-forming salts has also been evaluated. The lithium salt method is useful for accurate mass determination of these highly sensitive compounds. © 2012 by the authors.

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Bokros, A., Banfi, A., Kupihar, Z., Kele, Z., Illyés, T. Z., Szolomajer, J., & Kovacs, L. (2012). Electrospray ionization mass spectrometric analysis of highly reactive glycosyl halides. Molecules, 17(7), 8351–8358. https://doi.org/10.3390/molecules17078351

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