A versatile, inert atmosphere vacuum glove box

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Abstract

A research type, inert atmosphere vacuum glove box of stainless steel construction is described. The apparatus is suitable for a wide range of chemical and metallurgical applications as well as for physical property measurements on reactive samples. The design features a gas purification and recirculation system, automatic moisture monitoring system, and automatic pressure control system. A stereomicroscope with a long working distance to facilitate examination and experimentation on samples within the chamber is mounted over the chamber window. The vacuum glove box was designed to give a routine working environment of less than 1 ppm water and oxygen in argon. Mass spectrometric analysis on random samples of gas from the chamber has confirmed the operational efficiency of the apparatus. © 1969 The American Institute of Physics.

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Pack, J. G., & Libowitz, G. G. (1969). A versatile, inert atmosphere vacuum glove box. Review of Scientific Instruments, 40(3), 414–419. https://doi.org/10.1063/1.1683961

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