Solid-state NMR - a complementary technique for protein framework characterization

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Abstract

Protein frameworks are an emerging class of biomaterial with medical and technological applications. Frameworks are studied mainly by X-ray diffraction or scattering techniques. Complementary strategies are required. Here, we report solid-state NMR analyses of a microcrystalline protein-macrocycle framework and the rehydrated freeze-dried protein. This methodology may aid the characterization of low-crystallinity frameworks.

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Cerofolini, L., Ramberg, K. O., Padilla, L. C., Antonik, P., Ravera, E., Luchinat, C., … Crowley, P. B. (2022). Solid-state NMR - a complementary technique for protein framework characterization. Chemical Communications, 59(6), 776–779. https://doi.org/10.1039/d2cc05725e

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