Inconel 718 produced by hot pressing: optimization of temperature and pressure conditions

Abstract

This paper aims to act as a useful engineering tool for researchers who are studying the production of well-densified IN718 parts by uniaxial vacuum hot pressing. To the best of the authors’ knowledge, there is no relevant information on literature about densification of IN718 parts by this technique. This work is focused on understanding the influence of uniaxial vacuum hot pressing sintering conditions (temperature and pressure) on Inconel 718 (IN718) powder densification, microstructural, fracture mode, and hardness properties. The optimization of temperature and pressure sintering conditions are presented as well as its influence on the densification, microstructural features, and hardness properties. The sintering conditions included temperatures of 1000, 1068, 1150, and 1200 °C; pressures of 50 and 60 MPa; and a dwell time of 60 min. The results showed an increase in the grain size (GS) of the compacts with the processing temperature and a change on the fracture mode from intergranular dominant fracture to fully dimple ductile fracture. Regarding the microstructural properties, the results showed that γ′(Ni3(Al, Ti)) intermetallic precipitate originated from IN718 powders was retained in the sintered specimens. The hardness results revealed that the sintering temperature of 1000 °C is not enough to promote accurate densification. The optimum hardness results were achieved at 1200 °C (327 HV) with high levels of densification and pure intragranular fracture mode. In future studies, shear and tensile strength test should be performed in order to properly evaluate the mechanical behavior of hot-pressed IN718 specimens.