In this work, AlMgB14-based materials were produced from the intermetallic Alx Mgy powder and boron powder using mechanical treatment with a planetary mill and subsequent spark plasma sintering (SPS). Phase composition and structure of obtained materials were examined. Phase composition of sintered material is represented by the AlMgB14 phase (~95 wt%) and the spinel phase MgAl2 O4 (~5 wt%). The sintered bulk sample has a non-porous structure. The formation of the spinel phase is explained by the presence of oxygen in the raw boron powder.
CITATION STYLE
Zhukov, I., Nikitin, P., Vorozhtsov, A., & Boldin, M. (2020). Synthesis and characterization of ultra-hard ceramic AlMgB14-based materials obtained from AlxMgy intermetallic powder and boron powder by the spark plasma sintering. In Minerals, Metals and Materials Series (Vol. PartF1, pp. 313–317). Springer. https://doi.org/10.1007/978-3-030-36628-5_29
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