The microstructural evolution and mechanical properties of Zr-based metallic glass under different strain rate compressions

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Abstract

In this study, the high strain rate deformation behavior and the microstructure evolution of Zr-Cu-Al-Ni metallic glasses under various strain rates were investigated. The influence of strain and strain rate on the mechanical properties and fracture behavior, as well as microstructural properties was also investigated. Before mechanical testing, the structure and thermal stability of the Zr-Cu-Al-Ni metallic glasses were studied with X-ray diffraction (XRD) and differential scanning calorimeter. The mechanical property experiments and microstructural observations of Zr-Cu-Al-Ni metallic glasses under different strain rates ranging from 10 -3 to 5.1 × 10 3 s -1 and at temperatures of 25 °C were investigated using compressive split-Hopkinson bar (SHPB) and an MTS tester. An in situ transmission electron microscope (TEM) nanoindenter was used to carry out compression tests and investigate the deformation behavior arising at nanopillars of the Zr-based metallic glass. The formation and interaction of shear band during the plastic deformation were investigated. Moreover, it was clearly apparent that the mechanical strength and ductility could be enhanced by impeding the penetration of shear bands with reinforced particles.

Figures

  • Figure 1. Zr-based metallic glass nanopillars fabricated by dual-beam focused ion beam (DB-FIB) for in situ transmission electron microscopy (TEM) compression experiments.
  • Figure 2. (a) X-ray diffraction (XRD) pattern; (b) The electron backscatter diffraction (EBSD pattern of the as-cast Zr-based metallic glass.
  • Table 1. Yield stress of Zr-based metallic glass under different strain rates.
  • Figure 4. Variation of strain rate sensitivity with true strain as function of strain rate.
  • Figure 5. The SEM fractograph of Zr-based metallic glass deformed at a strain rate of 2.2 × 103 s−1.
  • Figure 6. SEM fracture surface of Zr-based metallic glass specimens deformed at strain rates of (a) 10−3 s−1; (b) 10−2 s−1; and (c) 10−1 s−1.
  • Figure 7. SEM fracture surface of Zr-based metallic glass specimens deformed at strain rates of (a) 2.2 × 103 s−1; (b) 3.2 × 103 s−1; and (c) 5.1 × 103 s−1.
  • Figure 8. TEM bright field images of a Zr-based metallic glass nano-pillar (a) before, and (b) after the in situ TEM nano-compression experiment; (c) the buckling position of a Zr-based metallic glass nano-pillar; (d) the EBSD pattern of Zr-based metallic glass after high strain rate deformation.

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APA

Chen, T. H., & Tsai, C. K. (2015). The microstructural evolution and mechanical properties of Zr-based metallic glass under different strain rate compressions. Materials, 8(4), 1831–1840. https://doi.org/10.3390/ma8041831

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