DAFS measurements using the image-plate Weissenberg method

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Abstract

An instrumental technique for DAFS measurements which can provide site-specific information is proposed. The approach uses (i) focusing optics with parabolic mirrors and a double-crystal monochromator, (ii) the Laue and Bragg settings and (iii) data collection by the image-plate Weissenberg method. Six image exposures are recorded per plate at five intrinsic energies and one reference energy. The single-crystal measurements were performed at the Co K-absorption edge, and the 200, 220 and 311 reflections of CoO and 511 and 911 reflections of Co3O4 were used for analysis. The regression analysis of χ(k), Fourier transforms of k3χ(k) and back-Fourier filtering have been performed.

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Sugioka, N., Matsumoto, K., Tanaka, M., Mori, T., & Sasaki, S. (1998). DAFS measurements using the image-plate Weissenberg method. Journal of Synchrotron Radiation, 5(3), 908–910. https://doi.org/10.1107/S0909049598000594

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