Color measurements of composite materials for tooth restoration in standardized in vitro conditions

Abstract

A national standard GOST R 58165-2018 (ISO/TR 28642:2016) 'Dentistry - Guidance on colour measurement' has been developed based on the international document which establishes standardized conditions for carrying out laboratory methods of measuring color by visual and instrumental methods. In vitro tests of samples of FiltekTM Ultimate, FiltekTMZ250 and Premise on the acoustooptic color analyzer SPEKTRON-M (FGUP 'VNIIOFI', Russia) in accordance with the recommendations of the standard GOST R 58165-2018 (ISO/TR 28642:2016) allowed to determine the effect of the shelf life of paste composite materials on the aesthetic indicators: colour compatibility, colour stability after aging and degree of transparency. The greatest changes in color characteristics in the CIELAB system during the storage of pastes were noted for the Premise Kerr A2 Enamel and A3 dentin composites. The greatest color change after exposure in water at 37 ° C was established for FiltekTMZ250 A4 samples with a long shelf life of the composite resin, ΔE=3.92>2.7 (p=0.001), but the color resistance of samples of the same composite from a new batch after exposure in water corresponds to the requirements of the standard, ΔE=2,18<2,7 (p=0,001).