A new efficient technique for Boc introduction into hydrazines and amines is reported. The substrate is stirred in molten di-(tert-butyl)dicarbonate without any solvent. The method requires neither DMAP nor other catalyst. The scope of the method is demonstrated using several hydrazines and amines.
CITATION STYLE
Raju, M., Mäeorg, S., Tšubrik, O., & Mäeorg, U. (2009). Efficient solventless technique for Boc-protection of hydrazines and amines. Arkivoc, 2009(6), 291–297. https://doi.org/10.3998/ark.5550190.0010.628
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