Efficient solventless technique for Boc-protection of hydrazines and amines

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Abstract

A new efficient technique for Boc introduction into hydrazines and amines is reported. The substrate is stirred in molten di-(tert-butyl)dicarbonate without any solvent. The method requires neither DMAP nor other catalyst. The scope of the method is demonstrated using several hydrazines and amines.

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Raju, M., Mäeorg, S., Tšubrik, O., & Mäeorg, U. (2009). Efficient solventless technique for Boc-protection of hydrazines and amines. Arkivoc, 2009(6), 291–297. https://doi.org/10.3998/ark.5550190.0010.628

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