A method has been developed for the preparation of US2 using UCl4, as a first step in the preparation of uranium monosulfide. The reaction of UCl4, A1 and H2S has been proved to be quite practical. It was confirmed by chemical analysis and X-ray diffraction analysis that almost pure US2 was obtained at temperatures above 400°C, and the conversion efficiency of uranium reached almost 100%. © Taylor & Francis Group, LLC.
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CITATION STYLE
Yoshihara, K., Kanno, M., & Mukaibo, T. (1967). Preparation of Uranium Disulfide from Uranium Chloride. Journal of Nuclear Science and Technology, 4(11), 578–581. https://doi.org/10.1080/18811248.1967.9732809