Direct conversion of chiral cyanohydrins to chiral nitrones by transimination

  • Hulsbos E
  • Marcus J
  • Brussee J
 et al. 
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Abstract

A new method for the preparation of enantiomerically pure N-benzyl nitrones is described. By using either a one-pot reduction-transimination or a one-pot Grignard addition-transimination sequence chiral O-protected α-hydroxynitriles can be converted into chiral aldo- and ketonitrones, respectively.

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Authors

  • Edith Hulsbos

  • Jan Marcus

  • Johannes Brussee

  • Arne Van der Gen

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