Traceless solid-phase synthesis of 2-amino-5-alkylidene-thiazol-4-ones

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Abstract

2-Amino-5-alkylidene-thiazol-4-ones bearing two diversity points are prepared by a solid-phase strategy exploiting rhodanine as the starting material. Rhodanine is first loaded on bromo-Wang resin, subjected to Knovenagel condensation with aldehydes, and cleaved off the resin in a traceless manner by means of an amine. © 2005 Elsevier Ltd. All rights reserved.

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Pulici, M., & Quartieri, F. (2005). Traceless solid-phase synthesis of 2-amino-5-alkylidene-thiazol-4-ones. Tetrahedron Letters, 46(14), 2387–2391. https://doi.org/10.1016/j.tetlet.2005.02.059

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