A relay route for the synthesis of azadirachtin

  • Veitch G
  • Beckmann E
  • Burke B
 et al. 
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Abstract

(Chemical Equation Presented) 22 Years in the making: Azadirachtin (1) was synthesized for the first time by a highly convergent approach, utilizing a Claisen rearrangement and a radical cyclization as key steps. End-game strategies relied on intermediate 2, which could be obtained by synthetic methods as well as by degradation of 1. Bn = benzyl, TBS = tert- butyldimethylsilyl. © 2007 Wiley-VCH Verlag GmbH & Co. KGaA.

Author-supplied keywords

  • Azadirachtin
  • Degradation
  • Natural products
  • Total synthesis

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Authors

  • Gemma E. Veitch

  • Edith Beckmann

  • Brenda J. Burke

  • Alistair Boyer

  • Carles Ayats

  • Steven V. Ley

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