Preparation of aluminum alkoxide by ethylene glycol

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Abstract

Aluminum ethyleneglycoxides, Al(OCH 2CH 2OH) 3 were obtained when aluminum powder mixed with AlCl 3 has been refluxed in dehydrated ethylene glycol at 471K for 12 h. Characteristics of the aluminum ethyleneglycoxide were measured by XRD and particle size distribution analysis. Particle morphology observed by SEM was like rectangular column shape. It is considered that the aluminum ethyleneglycoxides obtained is interpreted as corrosion product which is a reaction product that aluminum was corroded in ethyleneglycol.

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Seri, O., & Tanno, S. (2009). Preparation of aluminum alkoxide by ethylene glycol. Keikinzoku/Journal of Japan Institute of Light Metals, 59(8), 424–426. https://doi.org/10.2464/jilm.59.424

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