Journal Article

Synthesis of fluorous azodicarboxylates: Towards cleaner Mitsunobu reactions

Tetrahedron Letters (2002) 43(15) 2807-2810
DOI: 10.1016/S0040-4039(02)00322-2
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Abstract

The synthesis of a fluorous analogue of diethyl azodicarboxylate (DEAD) is described and preliminary results for its use in the Mitsunobu reaction given. Use of fluorous extraction methods have shown that chromatography is not necessary for reaction purification. © 2002 Elsevier Science Ltd. All rights reserved.

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Dobbs, A. P., & McGregor-Johnson, C. (2002). Synthesis of fluorous azodicarboxylates: Towards cleaner Mitsunobu reactions. Tetrahedron Letters, 43(15), 2807–2810. https://doi.org/10.1016/S0040-4039(02)00322-2

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