Thermal isomerisation of vitamin D3 in dimethyl sulfoxidet

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Abstract

Thermal isomerisation of vitamin D3 at 140 °C under nitrogen in the dark gave isovitamin D3 and isotachysterol as the principal products, identified by 1H and 13C NMR spectroscopy.

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Jin, X., Yang, X., Yang, L., Liu, Z. L., & Zhang, F. (2003). Thermal isomerisation of vitamin D3 in dimethyl sulfoxidet. Journal of Chemical Research - Part S, (11), 691–693. https://doi.org/10.3184/030823403322862941

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