Abstract
The use of KBr pellets in infrared spectroscopy has been investigated for monitoring solid-phase reactions. Synthesis of the methyl p-aminobenzoate on Merrifield resin (MR) is described as a model for this technique, which allows the progress of its three on-bead reaction steps to be monitored throughout their duration.
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Antonow, D., Graebin, C. S., & Eifler-Lima, V. L. (2004). An efficient monitoring technique for solid-phase reactions by KBr pellets/FT-IR using methyl p-aminobenzoate synthesis assisted by microwave radiation on Merrifield resin. Journal of the Brazilian Chemical Society, 15(5), 782–785. https://doi.org/10.1590/S0103-50532004000500028
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