Abstract
The total synthesis of oxyisocyclointegrin is described. The key steps in the synthesis included a Tsuji–Trost allyl migration to exclusively afford the corresponding monoallylated 1,3-diketone and a photochemical initiated oxidative cyclization to forge the oxepine core.
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Smith, R. J., Bower, R. L., Ferguson, S. A., Rosengren, R. J., Cook, G. M., & Hawkins, B. C. (2019). The Synthesis of (±)-Oxyisocyclointegrin. European Journal of Organic Chemistry, 2019(7), 1571–1573. https://doi.org/10.1002/ejoc.201801751
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