Abstract
A post-application of dry vortex grinding is used to improve a solid-state photodimerization to near quantitative yield that without grinding does not go to completion. Variable temperature X-ray crystal structure data support the vortex grinding to overcome detrimental effects of static disorder that suppresses the yield of the photoreaction in the solid.
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Elacqua, E., Kummer, K. A., Groeneman, R. H., Reinheimer, E. W., & MacGillivray, L. R. (2016). Post-application of dry vortex grinding improves the yield of a [2 + 2] photodimerization: Addressing static disorder in a cocrystal. Journal of Photochemistry and Photobiology A: Chemistry, 331, 42–47. https://doi.org/10.1016/j.jphotochem.2015.12.004
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