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New Applications of Crown Ethers. II. Synthesis of 4′-Formylbenzocrown Ethers

  • Wada F
  • Hirayama H
  • Namiki H
  • et al.
Bulletin of the Chemical Society of Japan (1980) 53(5) 1473-1474
DOI: 10.1246/bcsj.53.1473
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Abstract

4′-Formylbenzo-15-crown-5, -18-crown-6, and bis(4′-formylbenzo)-18-crown-6 were conveniently synthesized in excellent yields by Smith modification of Duff reaction: formylation with hexamethylenetetramine and trifluoroacetic acid or methanesulfonic acid.

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APA

Wada, F., Hirayama, H., Namiki, H., Kikukawa, K., & Matsuda, T. (1980). New Applications of Crown Ethers. II. Synthesis of 4′-Formylbenzocrown Ethers. Bulletin of the Chemical Society of Japan, 53(5), 1473–1474. https://doi.org/10.1246/bcsj.53.1473

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