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Synthesis, characterization and properties of a glycol-coordinated ϵ-Keggin-type Al13 chloride

Chemical Communications (2018) 54(33) 4148-4151
DOI: 10.1039/c8cc01363b
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Abstract

Herein we present the first example of a glycol-coordinated ϵ-Keggin Al13 chloride (gl-ϵ-Al13), which is the first chelated version since discovery of Al13 in 1960. The molecular structure consists of [AlO4Al12(OH)12(OC2H4OH)12]Cl7·H2O units with chelating mono-anionic ethylene glycol units replacing one bridging and one terminal oxygen site.

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Gu, B., Sun, C., Fettinger, J. C., Casey, W. H., Dikhtiarenko, A., Gascon, J., … He, S. (2018). Synthesis, characterization and properties of a glycol-coordinated ϵ-Keggin-type Al13 chloride. Chemical Communications, 54(33), 4148–4151. https://doi.org/10.1039/c8cc01363b

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