Synthesis and Adsorption Properties of Insoluble Starch Xanthate (ISX)

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Abstract

Starch xanthate was synthesized from corn starch and CS2 under alkaline condition. The effects of catalyst dosage, CS2 dosage and reaction temperature on sulfur content and copper ion removal rate were studied by single factor experiments, and the structure of the product was characterized by FTIR, SEM and XRD. The results showed that the optimum synthetic condition of ISX was NaOH dosage 16 mL, CS2 dosage 2.5 mL, reaction temperature 35 °C and reaction time 2 h. The sulfur content of ISX synthesized under this condition was 7.54%, the removal rate of copper ion was 90.5%, and the adsorption capacity of ISX was 90.0 mg/g.

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Li, H., Zhang, L., Gao, Y., & Liu, Z. (2020). Synthesis and Adsorption Properties of Insoluble Starch Xanthate (ISX). In IOP Conference Series: Materials Science and Engineering (Vol. 735). Institute of Physics Publishing. https://doi.org/10.1088/1757-899X/735/1/012026

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