Abstract
(Sulfodifluoromethyl)phosphonic acid, (HO)2 P(O)CF2SO3H, has been synthesized for the first time. This mixed phosphonic-sulfonic acid was prepared from (C2H5O)2P(O)CF2SO3Na, which had been synthesized via oxidation of the corresponding sulfinate salt, (C2H5O)2P(O)CF2SO2Na. The sulfinate salt was prepared from (C2H5O)2P(O)CF2X (X = Br, I) and [(C2H5O)2P(O)CF2SO2]2Cd precursors. © 1989, American Chemical Society. All rights reserved.
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CITATION STYLE
Burton, D. J., Modak, A. S., Guneratne, R., Su, D., Cen, W., Kirchmeier, R. L., & Shreeve, J. M. (1989). Synthesis of (Sulfodifluoromethyl)phosphonic Acid. Journal of the American Chemical Society, 111(5), 1773–1776. https://doi.org/10.1021/ja00187a033
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